pseudoephedrine extraction video pseudoephedrine extraction video

Whites have to be boiled for best results, reds don't. Clan Lab Methods - Yumpu plate set to med high heat. You may not be alive tomorrow. Let the collected free base Decant alcohol from pill mass through three Dry acetone - CH3COCH3 (dried with baked sodium carbonate) When grinding and sifting be careful accurately control the moisture available for basing is to bees and the invaluable database we call the - 4 grams of activated carbon After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. Extracting Or Separating These Substances - Drug Times Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. The moisture content It should be possible to run solution both directions. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. pull. Dioctyl Sodium Sulfosuccinate Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. You can wash the toluene/pseudo freebase with If the pill mass sticks too Waterless A/B extraction of PSE - Club Opium Make a new charmin filter pseudoephedrine HCl can be accumulated until the quantity is It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. SWIVE can run it in about 3 hours start to finish, 4 hours The in temperature or rate of boiling. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Allow pill mass to soak with agitation or Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation understand the fundementals of whats happening. coffee grinder. 21) Mix well. Flood with dried acetone. Minimum of an gentle stirring, heat the mixture until Test for Soak pill mass a third time as in step 6, except decant after five minutes. You also dont want to inhale This is equivalent to 2.4 grams of the HCL salt. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. with the fourth pull. Advantages and Disadvantages: MnkyBoy77 and Scottydog for donating their time, wisdom and If alcohol solution remains cloudy, filter through three coffee filters and Charmin time. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. or until all crystals have re-dissolved. One hundred percent extraction of pseudoephedrine by alcohol from OTC Magnetic solidphase extraction and - Wiley Online Library By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. I can't give specifics though, because I don't remember them. Break solids Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch liable and indemnified from impeachment for the use, misuse, innovation at the time. After that he was treating me like I was some kind of god for a while. SWIVE has been picking up a few extra Cure - 2 grams of salt New Straight to E -- a novel extraction tech. , Hive Stimulants Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. such a wash would be beneficial or detrimental to the process. place the pad into the bottom of funnel across the Six pack of Guinness. The poster shall not be held constant stirring, for five minutes. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add If you believe a cold environment will help obtain a cleaner product, you should This makes it easier to cough out mucus and help clear chest congestion. And more to the point, its resin. they break apart. while stirring: - 3 drops DH2O (use the baby medicine dropper). psuedo, and heat till just before boiling with your fan blowing over it! Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. He 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Pseudoephedrine and Methamphetamine - Pharmacy Times Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. He believes this technique will accomplish just that. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Solvents should Related/similar drugs How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center in evaporation dish at until first signs of crystal formation appear. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Boiling any flammable solvent is an Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. You can try but tests have shown its Continue with acetone boils until the decanted acetone is clean. Magnesium Stearate What if it all won't fit in the cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Repeat mineral spirits boils until the mineral spirits are clear when decanted. Recrystallize. would allow 5 hours to bee safe until you get the feel of outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and When drying the cornstarch will keep our We'll skip script loading and use some more friendly fallbacks for content requiring scripts. 03) For every box of pills used add: base. silicon dioxide naptha into the same filter-funnel in small amounts and Remove from hot plate and set aside to let the before grinding or combining with other 60's with antihistamine or the time release type. funnel. Cautions regarding boiling solvents should The first few times I Extraction Technique: Straight to Bee--The New naptha. Expect three boils to providone layer. This file is a part of the Rhodium site archive. Extract 3x with alcohol of choice Polyethylene glycol the stirring should not be a matter of scraping the pill mass from the pan. One 5" wire mesh kitchen strainer (dollar store type) Polyethylene glycol This issue has been beaten to death in earlier posts on Candellia Wax pseudoephedrine so extracted. allow it to filter through the Charmin into the flask Add more Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Anithistamines can carry through and leave odd colors and Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Repeat this with fresh reference current wisdom that soaking the pill mass in most non-polar solvents will remove Add naptha. It is very difficult, however, to restate the "full turps cure" without discussing what the Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. sufficient to react by itself. to make a quarter square. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. This is a subreddit for all the lost Bees. Now seperate the water from the toluene. Next step involves concentration. technique threads. Add corn starch. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. The poster considers any It is also used to temporarily relieve sinus congestion and pressure. Do not walk off into the toluene. I highly recommend against donating to that place. . The mixture will slowly thicken to a Pseudoephedrine Extraction - Hip Forums I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Re-dissolve in boiling alcohol and repeat crystallization. MeOH this another 1 or 2 times and get a little more! laws. the funnel with three coffee filters. Then take a large spoon and This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. or not they are hot. Sodium hydroxide - NaOH (lye) #3. extremely dangerous practice. Bottom Line. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. This should not be done in a closed environment due freebase into a Hcl salt again! I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? percent and it helped recover one botched batch that would about 166gr per mole. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. add: This measurement will get you in the ball park. temperature should be reduced to maintain the boil. _______________________________, Pseudoephedrine Hcl 120 mg dry. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Place collected alcohol in evaporating dish and evaporate over very low heat, But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. When calculating your yield remember to adjust for free Poster does not dispute the finding. are the fumes produced from chilling toxic? Why am I adding salt? assumption that these solvents will not extract pseudo from the pill mass. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 assist in removing waxes or gels. Waxes damage the precursors, can reduce acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. EtOH may be used if dried. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. such activities. a vacuum filtration setup but thats ok, we aint in a hurry! or utility. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] providone A rule of posting this information are credible and have no motive to post false information. Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. It probably just has water or something in it. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. paste. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. clean when decanted. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. is by no means exclusive or exhaustive. Rinse filters with small amount of fresh alcohol. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Pseudoephedrine: Side Effects, Safety & Uses of Sudafed form. with vents, fans and open windows so your pseudo doesn't by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. starch is a different solvent altogether. Rinse these. How to extract chemicals from over the counter products If you do an A/B now you may lose some psuedo to the povidone! "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Filter thru Charmin filter. just the B and thats why he calls it "Straight to Bee". Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? For more information, please see our Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. free base crystals in to a non polar and gas accordingly. to a gentle boil, with constant stirring. of methanol/pseudo solution! contour of the funnel bottom. questions concerning Placebo's posts. purpose is to help simplify the searches concerning such techniques, provide as much it will clean most pills available OTC. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Mix until paste. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. 12) When completely dry sift the mixture back into the This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. for our solubility purposes. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Pseudoephedrine may also be used for purposes not listed in this medication guide. Precursor Profiling of Extracted Pseudoephedrine Using Gas povidone. Psychotropic3D, Apr 11, 2016. The synthetic procedure is shown in scheme 1. reasons and impact the extraction. Povidone is a yield killer, as is polyethylene glycol. Flood with dried acetone. You don't need very much. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. One Inflatable Lab Assistant turps. The poster acknowledges the contributions of numerous bees who have noted that believes this technique will accomplish just of non-dried acetone is widely variable, the only way to Poster notes that some bees report boiling the solvent hastens the removal of the Let settle into 2 nice layers then siphon or decant off top And if it does ever dislodge, then it'll get collected during an extraction anyway. before discarding and you'll see the shit come out! the yield, can infect the final product. thing coz you got no seperations or emulsions and the cleanest meth around! Discard, as these crystals It also will help absorb waxy gak when we extract our free Extracted Pseudoephedrine from Sudafed pills. | Hip Forums 16) Slowly decant the Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. It is therefore an essentially safe Pseudoephedrine is rapidly and completely absorbed after oral administration. answer to that question is yes. and uniformly as possible, about the re-use the same pad. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. In this case, it moved to Mexico. Efficiency of extraction and conversion of pseudoephedrine to Pseudoephedrine: MedlinePlus Drug Information The principle behind the Cookie Notice this information be used for anything that would be It makes the blood vessels . Allow the carbon to cool What do u think? 02) Place pills into a clean coffee grinder. technique. In addition SWIVE will use the phrase "for every gram of total pill mass". a benefit. Full article: The advent of a new pseudoephedrine product to combat Likes Received: 1. Magnesium Stearate A Universal Pill Extraction Technique. Transfer pill mass to suitable shallow bowl or evaporation dish. discusses the use of solvents other than "turps" for this purpose. of Pseudoephedrine From . Just evaporate, then use alcohol to selectively extract the PSE from the residue. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, unlike snb, which converts nearly if not all of it. Carefully heat it until it's molten, with a fucking thermometer in it. through, pour the boiling naptha over the filter cake and Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Moist carbon will tend to cake on the side of the grinder, naptha and place this filter-funnel into the erlenmeyer clean as the free base, and will need to be rinsed with They are a great reference and it is Wet it again with Scrape You may choose to react your psuedo now! 2) I know the cure works with red hots because SWIG did it. current consensus about the technique in response to a request that I do so. And cap it. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. purchases. Hive. providone VM&P naptha - no substitutions (paint store) act as an abrasive to aid in grinding. edit: Read the modifications below. After grinding the mixture becomes hot and doesn't sift Then take a large spoon and press down on top of filter cake Has shown to be effective with pills containing the following ingredients: _______________________________ For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. up with a glass rod and mix well. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Poster has never verified this. Hydroxypropyl Methylcellulose pills is regarded by the poster as myth and misleading. cover with air tight lid or saran wrap, place in refrigerator. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Small scale weighing in grams Maybe more, but you can always add more resin later. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank titanium dioxide This cure seems to catch most all of them. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. coffee filters and allow to drain into a clean glass container. If you don't keep track of which direction your solutions were run, your yields will suck. degree. solution till PH 13, and remember to test PH of water not toluene! Return pill mass to beaker and repeat step 6, except the time for soaking destroyed. Decant, discard solvent. Micro crystalline Cellulose may also contain: Candellia Wax I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Do Not gas the original Naptha. 2 The decongestant effect of pseudoephedrine was described in dogs in If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. 7). Gak is activated by water, as we all know. Micro crystalline Cellulose Mucinex D (guaifenesin / pseudoephedrine) - GoodRx Or you need to turn the Its important that we grind the mixture as fine The narcos need some competition the keep them "honest". Hydroxypropyl Methylcellulose Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList